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Biodentine is a tricalcium silicate cement used as a dentin replacement in restorative dentistry. The aim of this study was to assess the influence of cavity moisture on the immediate sealing and morphology of the interface between Biodentine and the dental tissues. 20 class II cavities were prepared in extracted teeth. 10 cavities were dried using the air spray before restoring with Biodentine and 10 cavities were preserved moist for the restorative procedure. The teeth were subjected to a microleakage test and then the axial sections were observed under optical microscope and scanning electron microscope. In most situations Biodentine provided an immediate good marginal sealing and a tide contact with adjacent tissues in both occlusal and cervical margins which did not seem to be influenced by the moisture of the dental supporting tissues.

Changes in the surface roughness of dental restorative materials after tooth brushing are inevitable. The abrasion is known to increase the possibility of dental plaque accumulation which is responsible for several pathologies of the oral cavity. The aim of this in vitro study was to evaluate the changes of surface roughness of microhybrid composite materials produced by different toothbrushes with and without toothpaste. Forty-eight specimens of two composite materials (Charisma and Super-Cor) were prepared using a silicone template according to the manufacturer’s instructions. Each sample was brushed for eight hours. Each group of specimens was divided in two subgroups: half of the samples were brushed using only distilled water and the other half with a mixture of distilled water and toothpaste (Colgate Total; ratio 1:1). The average roughness value (Ra) of surfaces were measured with profilometer three times: the initial measurement was performed before starting the toothbrush simulation, the second was after 4 hours and the third was after 8 hours of brushing. Three different bristle stiffness toothbrush heads were used (medium sensitive, medium and soft). After collecting all numerical data one-way ANOVA and Friedman tests were performed for statistical analysis. All examined microhybrid composites exhibited changes in surface roughness after the toothbrush simulation. The simulation of toothbrushing without toothpaste, only with water as cleaning substrate, showed at every measurement the lowest values of roughness in all three toothbrush heads. Significantly increase of mean Ra values were observed in both tested composite samples when medium and soft toothbrushes with toothpaste were used. The surface roughness changes of tested microhybrid composites depend on the brushing procedure. The toothpaste has a much greater effect on the abrasion than the type of toothbrush.

The brake pads are one of the basic components for the development an ecological transport. The main objective of the paper is to produce green brake pads used shells as filler material capable to reducing the emission of fine and ultrafine particles resulting from vehicle braking systems. The stages in the development of this goal were: establishing the chemical composition of shells, formulating the recipes of composite materials, selecting parameters of technology, obtaining in laboratory and characterization of new materials in terms of physico-mechanical and tribological characteristics, evaluating their performance compared to similar materials presented in the scientific literature.

The purpose of the present study was to evaluate the mechanical parameters at compression tests for two different restorative composite resins. The materials here under study were: Gradia Direct (GC Corporation, Tokyo, Japan) and Filtek Ultimate Universal Restorative, (3M ESPE, St. Paul, MN, USA). 30 cylindrical samples, 15 for each material, with a thickness of 6 mm and a diameter of 5 mm, were made. The compression behavior at mechanical tests for each sample was analyzed. One-Sample Kolmogorov-Smirnov Test followed by Paired Samples t-Test was used for statistical analysis and determining the level of significance. Gradia Direct had a lower value of Young’s modulus than Filtek Ultimate Universal Restorative, the results being statistically significant (p = 0.001 [ 0.05). The comparative evaluation of the compressive strength did not reveal statistically significant results between the two materials (p = 0.098 ] 0,05). Regarding the compressive strain the values were significantly lower for Filtek Ultimate Universal Restorative (p=0.000 [ 0.05). The microhybrid composite evaluated in the present study proved to have better mechanical properties than the nanofilled composite.

Elastomeric chains, as means of force delivery, are one of the most studied elements of the orthodontic field. Effects on tooth movement are closely related to force degradation degrees of these polymers. Unfortunately, due to varied manufacturing techniques and materials, different brands of elastomeric chains offer different initial force values and different force decay, with direct impact on tooth movement duration and effectiveness and quality of orthodontic treatments.

The aim of this work was the development of a series of glass fiber reinforced composites (FRCs) for CAD/CAM applications in dentistry and the characterization of their structure by SEM, Raman and FTIR spectroscopy. A selection of 2 different types of resins (R1 composed from 25%Bis-GMA, 40%UEDMA, 35% DMTEG and R2 composed from 65%Bis-GMA, 35% DMTEG) with 2 different types of hybrid filler (F1 with 42% quartz, 42% radiopaque glass and 16 % hydroxyapatite and F2 with 90% quartz and 10% colloidal silica) and 3 different types of E type fiber glass geometries (veil 30g/m2, twill 163g/m2 and textile 300g/m2) in 4, 6, 8 and 10 layers were used in this in vitro study. Raman analysis, showed a powerful interaction between the polymer and the fiber glass. FTIR and SEM data revealed that the different fiber glass geometries were well incorporated inside the resin, resulting an acceptable homogeneity. Within the limitation of this study, it is possible to achieve a fiber glass reinforced composite for the use of CAD/CAM technology. Further investigation must be done in order to test all the properties of the new material.

Materials used in additive techniques are initially in a plastic state to be inserted into different cavities or easily molded (a blunt, for example), after which they pass into a rigid phase. This process is carried out by various methods depending on the material nature. The process can be purely physical (solidifying the alloy melt, the termoplasticized macromolecular compounds), modification and rearrangement of the internal structure (sintering of ceramic masses, crystallization of glasses, amalgam intake), a process of evaporation of some components (lacquers, plasticizing polymers) or a chemical process. This latter process can be an acid-base reaction between two inorganic substances (PCZ, CIS cements), a chelating reaction (ZOE cements) between a phenolic range (organic compound, usually eugenol or orthoethoxybenzoic acid) and an inorganic powder (ZnO) or a reaction in which a macromolecular compound is formed. After the type of the reaction, the macromolecules are classified into polymers (the formation reaction is called polymerization, the compounds of which are obtained by monomers, the main chain is formed by the carbon atom only), polycondensates (the formation reaction is called polycondensation, the chain also formed from heteroatom-ON, depending on the type of material) or substances that are obtained by polyaddition ( a repeated addition, the mechanism being different from the polymerization. Our study was conducted in the Dental Clinic and comprises a total of 17 patients. The group was represented by patients aged 50-85 years. Clinical observations have been made on cases of fracture of acrylic bases, with the analysis and assessment of some clinical aspects with increased risk of fracture (jaw / mandible, median / paramedian fracture line, etc.), which increase the risk to and fracture when associated. Clinical observations have shown the presence of the risk of fracture in acrylic prostheses, with the need first of all for the proper design and realization of mobile prostheses, but also for the use of inserts.

Successfully used in bone surgery for more than 65 years, self-hardening organic cements (CCOs), in particular acrylic cements, are today, the most advanced complementary biomaterials used in articular endoprosthesis. One of the strategies for obtaining of performing anchorage of artificial implants is to develop new acrylic cements with improved physical, chemical and biomechanical characteristics. The aim of this paper was to identify the compositional and morpho-structural changes of acrylic cements induced by the composition of the liquid phase of the material. Such changes influence the potential to generate the physical bonds responsible for fixation and stabilization of endoprosthesis. The samples studied had different compositions due to the mixture of acrylic monomers, methyl methacrylate (MMA) and butyl acrylate (BuA) in the liquid component of cement. The MMA / BuA ratio varied between 1/0 v / v and 1/4 v / v. Changes in the composition and morphology of cement samples have been highlighted by ESCA (Electron Spectroscopy for Chemical Analysis), EDX (Energy-Dispersive X-ray Spectroscopy), IR spectroscopy and SEM images. The obtained data show that minor changes in cement composition can significantly influence morpho-structural characteristics such as pore size and their distribution in the mass of fixing material.

The thermoplastic materials studied are biphasic. They consist of a polymer mass and a short glass fiber, the percentage being between 10 and 30%. We have shown, both analytically and graphically, the evolution of wear occurring on the steel surface in contact with glass fiber-reinforced polymers. The evolution in time of this process depends on the evolution of the friction coefficient in the process of the dry linear contact between different polymers and different types of steels. We have made a connection between the theoretical case and the experimental results. The experimental method used was the wear imprint method through which the wear depth and wear volume were determined. The wear process is complex and is accompanied by adhesion and corrosion phenomena. Any modification of the input parameters such as speed, temperature, load, quantity of glass fibers in the polymer lead at a certain one evolution of the wear behaviour of the composite material.

This paper presents the results of an investigation into the structure and properties of intraocular lenses (IOL) that are available on the ophthalmological market. The majority of implants of this type are based on acrylics or poly(methyl methacrylate) (PMMA). The acrylic lenses can be curled, which allows the making of just a minor incision during the associated implant surgery. The drawback of PMMA implants is their high rigidity, resulting in the need for a larger incision during the implant surgery. The benefits accrued from wearing such an implant are (1) the correction of focus for clear vision and (2) protection of the retina against UV-A radiation. X-ray diffractometry has confirmed the amorphous structure of all of the lenses investigated in this paper. The absorption and transmittance of the selected implants have been measured; differences found in the directional values of the transmittance and absorbance suggest the presence of differences in the implant coating (such as: different thickness or lack of coating on one side). It has been found that the PMMA-based implants exhibit the better properties with a level of light transmission in the visible spectrum of almost 40% and total protection against UV radiation. The acrylic implants feature lower transmittance in the visible light spectrum, and two of the investigated acrylic lenses failed to provide adequate protection against the UV radiation.