The aim of this study is to investigate the effect of polishing with different solutions on the surface roughness and hardness of two different polymethylmethacrylate temporary restoration materials. In the study, two different temporary crown materials prepared in the CAD / CAM system and prepared by the traditional method were used to test a total of 224 pieces of 10 mm diameter and 2 mm thickness. After the surface roughness and micro hardness values were measured, samples were randomly divided into seven groups among themselves; After waiting 24 h, 1 and 3 weeks, values were measured again. Data were evaluated using 3-way analysis of variance (ANOVA) and Tukey HSD test. The temporary restorative materials` surface hardness and roughnesses are important to be able to stay in oral cavity without any changes. And it is also important to determine which of the materials (prepared by temporary conventional materiels or by the CAD/CAM) are less effected by the liquids in oral cavity.
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High and low density polyethylene materials constitute about 48% of total weight of plastics waste in Europe, that depends on the frequent use of these materials in packaging applications. This paper analyze the recycling effect on the mechanical properties of high and low density polyethylene (HDPE and LDPE). A mechanical recycling process was tested for the plastics waste of high and low density polyethylene, then a tensile and impact tests were performed on different mixing ratios for each of the both materials ranging from 100% of the virgin material and up to 100% of the recycled material with a difference of 10% of the sample to the other. This paper discusses the tensile properties of tensile stress at the fracture, elongation and modulus of elasticity and the impact test results for HDPE and LDPE were compared with each other.
Kenaf is a nonwoody fibrous plant, and its fibre can be potentially used as a reinforcement in the matrix to produce biocomposite materials. The properties of biocomposite materials are highly dependent on the reinforcing material and the matrix used as a binder. This study used kenaf fibre as a reinforcing material with different compositions (10, 20, and 30 wt.%) and different fibre lengths (1 cm and 3 cm) in the matrix using the casting process. Low viscosity epoxy resin (635 thin epoxy resin) with a viscosity of 6 poise was used as the matrix. The results showed that the highest flexural strength, impact strength and shore hardness were obtained at a 30 wt.% kenaf fibre composition with a 1-cm kenaf fibre length, namely, 85 MPa, 338 KJ/m2 and 98 SHD, respectively. The length of the fibre in the matrix affects the mechanical properties of the resulting biocomposite. This condition is caused by kenaf fibres with a length of 1 cm being more dispersed in the matrix than fibres with a length of 3 cm.
Glass reinforced plastic, so called GRP, is a composite material made of glass strands called fibbers woven together to create a flexible fabric. GRP is a lightweight material with many and diverse applications ranging from the manufacture of reservoirs for different liquids to the manufacture of boats, yachts, chairs and even children playground furniture. The behaviour of this material under static and dynamic loads is still raising interest from the scientific community and a large number of researchers. This continued interest is due to the material versatility for different applications depending on its manufacture process that has a significant weigh-in in the material mechanical properties. These resulting mechanical properties need to be carefully analysed and benchmarked prior to using the obtained material in commercial applications. The scope of this research study is to analyse the behaviour of glass reinforced plastic plate panel with reinforcements on one and two directions under static and dynamic loads employing both experimental and numerical methods for results validation. The methods used in this research study for the dynamic loads can also be applied successfully to other composite materials. Additionally, the stress plots have been analysed in iteration in order to ensure the most optimal reinforcement pattern.
Thermoplastic materials have great usage through FDM 3D printing technology. Today, FDM 3D printer is available to the broad population, and some of the thermoplastic materials is widely used due to their small price and availability. Such thermoplastic materials are ABS (Acrylonitrile butadiene styrene) and PLA (Polylactic acid). In this paper the possibility of drone frame design optimization that can be made from ABS and PLA plastics using FDM 3D printing technology is analyzed.
In the medical field the additive manufacturing process by fused deposition modeling has gained a great importance given the ability to create complex, organic geometries, in a short time period and the possibility of high customization. By fused deposition process the part is created layer by layer and the resulting part is characterized by high anisotropy, dictated mostly by printing parameters. To alleviate the anisotropy and to study the mechanical behavior of the 3D printed parts thermal processing is used. The materials used as filament is a poly (lactic acid) with copper particles embedded for antibacterial purposes. Samples were 3D printed using a commercial printer, thermally processed and tested in compression. On the failed specimens fracture investigations were performed to understand mechanical behavior during compression. The mechanical characteristics showed improvement and the anisotropy decreased as the processing temperature increased, but the samples became brittle. The mechanical behavior changed drastically on the thermally processed samples because of structural changes: a discontinuity between exterior layers and infill layers was created post layer fusion, the first region being the one stressed and failed first during tests.
In order to place a product on the market that is completely safe for users, the manufacturer must go through certain steps: design, prototyping, execution and prototype validation through experimental methods, obtaining documents that allow to sell the product from certain public or private companies (for example homologation certificate) and series production. One of the most important steps is the validation tests of the prototype because it will depend on them that the prototype corresponds to the design requirements.
Obtaining parts made of composite materials through 3D Printing Additive manufacturing have fully proved their usefulness due to a number of advantages such as: the possibility to directly create complex shapes without going through the classic process of transforming the semi-finished products into finished parts through technologies which consume resources and energy and are totally unfriendly to the environment. The main disadvantage of the parts made by 3D Printing technologies is that they are less resistant from a mechanical point of view. This was solved with the emergence of the 3D printers capable of printing composite parts consisting of a plastic matrix reinforced with continuous fibers. This research focuses on studying 4 types of composite materials from the point of view of their mechanical properties: Onyx - a rigid nylon in which micro carbon fibers are inserted and Onyx reinforced with carbon, fiber glass or kevlar. Standardized specimens were made for the uniaxial tensile test and the experimental program was designed evaluating: the Elastic modulus [GPa], the Maximum Tensile stress [MPa], the Tensile strain at maximum Tensile stress [mm/mm]. The principal strains were also determined, by means of the digital image technique made using the Aramis system from GOM. The experimental tests confirm that these new materials will be serious candidates to be used in the engineering applications in various fields.
In time the environmental conditions could damage textiles (materials/ artifacts) causing the need to develop better non-destructive or at least micro-destructive analysis techniques of the samples. There are ethnographic textile artifacts that were treated in the past with various pesticides, that have not been mentioned in any document. These are often re-treated with chemicals by museum staff as a method of preventing pest infestation. Due to the progressive use of many pesticides, this paper was focused on the detection and quantification of three pesticides: malathion, methoxychlor, and permethrin (cis- and trans- isomers). Gas chromatography is one of the most widely used analytical techniques for characterizing volatile organic compounds and therefore was the analytical method of choice for the present study. Because these analytes are found at trace levels, the detection and quantification limits of analytes are very small and it is necessary to optimize and validate a SIM method - that allows the mass spectrometer to detect specific compounds with high sensitivity. In SIM mode, the instrument is set to collect data at selected masses of interest, thus increasing the accuracy and precision of the quantitative results. The present paper is aimed to develop this type of method with specificity and selectivity, high precision (expressed in terms of repeatability and intermediate accuracy), accuracy, suitable working range and linearity, and high degree of series’ homogenity.
The effect of mold conditions was investigated in terms of mold temperature (30oC and 90oC) and cooling time (30 s and 60 s) on the heat resistance of injection-molded bars for stereocomplex polylactide-b-polyethylene glycol-b-polylactide (scPLA-PEG-PLA). Comparative study was performed for poly(L-lactide) (PLLA) and PLLA-b-PEG-b-PLLA (PLLA-PEG-PLLA). scPLA-PEG-PLA was 90/10 (w/w) PLLA-PEG-PLLA/poly(D-lactide) blend. scPLA-PEG-PLA exhibited the easiest crystallization upon cooling scan as shown by differential scanning calorimetry (DSC). Higher mold-temperature and longer cooling-time induced higher degree of crystallinity as assessed by X-ray diffractometry (XRD) except for PLLA bars. The heat resistance of both PLLA-PEG-PLLA and scPLA-PEG-PLA bars was improved with increased mold-temperature and cooling-time as shown by dynamic mechanical analysis (DMA), vicat softening temperature (VST) and heat distortion-resistance tests except for PLLA bars. In conclusion, the heat resistance of injection-molded bars prepared at 90˚C mold temperature was in the order scPLA-PEG-PLA ] PLLA-PEG-PLLA ] PLLA. The results suggested that flexible PLLA-PEG-PLLA and scPLA-PEG-PLA with high degrees of crystallinity were successfully obtained by injection molding for use as good heat-resistant bioplastic products.