HORIA PLES, COSMIN SINESCU, LUCIAN FLOREA, FLORIN IONEL TOPALA, LAURA CRISTINA RUSU, DRAGOS NICOLAE CIRES, ADRIAN PODOLEANU Plastination Biopsy Samples from the Central Nervous System as a Solution for Time Domain Optical Coherence Tomography Noninvasive Investigation Method
A biopsy sample that was taken from neurosurgery then introduced into the solution of formaldehyde was examined with Time Domain optical coherence tomography. The results are inconclusive and so that preserving was accomplished by plastination the tissue sample in which the degree of rigidity of the sample is controlled without destroying the tissue. Keywords: Plastination, Optical Coherence Tomography, nervous system
ELENA BERCU, ION SANDU, CEZAR-DORU RADU, VIORICA VASILACHE, VASILICA TOMA, HORIA-ADRIAN ALDEA Influence of Anionic Maleic Polyelectrolytes on the Colour Parameters at Dyeing the Melana Types Fibres with Crystal Violet
The present study pursues the influence of polyelectrolytes based on maleic co-polymers with styrene (NaM-S) and vinyl acetate (NaM-VA) under the form of natrium salt, on the colour parameters CIE L*, a*, b* of the Melana-type polyacrylonitrile fibres dyed with Crystal Violet. The colour differences are ascribed to the modifications appeared in the colour components, in terms of concentration, polyelectrolyte character and tinctorial parameters: dyeing duration and temperature. Keywords: maleic anionic polyelectrolytes, Crystal Violet, Melana - type polyacrylonitrile fibres, colour parameters CIE L*a*b*
The Kinetics of Consumption for Some Phenolic Antioxidants at the LDPE Thermooxidation
The kinetic approach on thermal stabilization of LDPE in the presence of 7 chalcone compounds is presented. The application of zero order or first order treatment to the experimental date obtained for stabilized LDPE has revealed that the depletion of antioxidant is a first order process. The comparison of the most efficient member of chalcone series and some commercial phenolic antioxidants has provided the following sequence for the prevention of oxidation: ETANOX – 330 ] D4 ] IRGANOX – 1076 ] CYANOX – 2246 ] TOPANOL – OC ]] purified LDPE
Studies on the Rheological Behaviour of some Retarding Additives for the Concrete of Wells
Rheological behaviour of some products based on chemical modified starch, with characteristics proper to retarding additives for concrete designed for cementation of the big depth wells, was investigated. With that end in view, rheological tests of several pastes obtained from products of the hydroxypropylstarch type were carried out. Maintaining, at pastes preparation, the concentration of 10% additive, proved as being the most efficient in use, shearing strain tests were performed at 20°C, 40°C and 60°C versus keeping time of pastes, namely, 24 h and 48 h from preparation time. At the same time, influence of the disodicphosphate and urea additions over rheological pastes was investigated versus the same parameters. Based on the experimental results obtained, the mathematical models describing rheological behaviour of the tested additives, within a large range of external stress and temperature, were elaborated.
The Bismaleinimide - an Agent for Oreventing Destructive Processes
This paper presents data concerning the capacity of a bismaleinimide (BMI) to protect elastomers with different structures and unsaturated degree and the copolymers EVA submitted to thermooxidative destruction at 80 - 200ºC. The main structural changes were followed in the IR domain and the kinetic parameters of the processes were determined.
Considerations Regarding the Compatibility of some Rubber Structures with Leather Wastes
The research investigated the compatibility between the styrene-butadiene rubber mix and wastage materials of finite cromated leather in order to obtain products necessary in various industries or specifically in the leather and shoes industry. The researchers immersed multiple composite samples containing rubber and various proportions of leather-wastage in three solvents: benzene,carbon-tetrachloride and cloroform. The samples where then monitored during their expansion in time and the changes that occurred in the IR spectra. The studies have demonstrated the material compatibility confirmed also by mechano-physical determinations.
The Influence of the Chemical Structure of the Acrylic Polymer on the Properties of the Coated Materials
Five commercial products, based on acrylic polymers, have been used for cotton coating. The structures of the polymers have been established based on their IR spectra of the active compound from the acrylic dispersion. The properties of the coated materials have been discussed in connection with the structure of the acrylic polymer.
Fucntional Poly(Succinimide-ethers)
New poly(succinimide-ether)s with maleimidic rings in the side chain were synthesized by a chemical modification reaction on the polymers containing hydroxylic pendant groups. The polymers were obtained in good yields and they were characterized by elemental analysis, infrared and proton nuclear magnetic resonance spectroscopy, gel permeation chromatography, dynamic thermogravimetric analysis and solution viscometry.
Synthesis of Aminophosphonates Grafted on Styrene Divinylbenzene Copolymer
A simple, efficient and general one-pot method has been developed for the synthesis of aminophosphonates grafted on styrene-divinylbenzene copolymers from benzaldehyde grafted on styrene-divinylbenzene copolymer with amines and diethyl phosphite in tetrahydrofuran. The aminophosphonates grafted on insoluble macromolecular supports were characterized by infrared spectroscopy, thermogravimetric analysis and scanning electron microscopy. Keywords: aminophosphonate groups, stirene-divinylbenzene copolymers
Organic Coatings Based on Powder Dyes. I. Thermoplastic Powder Dyes
Coating powders are finely grounded polymeric materials containing binders, pigments, extenders and special additives, used to obtain decorative and protective organic coatings. There are two major categories: thermoplastic and thermoreactive coating powders, based on thermoplastic and on thermoreactive binders, respectively. This paper presents the classes of thermoplastic coating powders, and their main characteristics.