Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides

Mitran, Elena-Cornelia; Sandulache, Irina-Mariana; Lite, Cristina-Mihaela; Radu, Lucian Gabriel

Elena-Cornelia Mitran, Irina-Mariana Sandulache, Cristina-Mihaela Lite, Lucian Gabriel Radu

Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides

Abstract:
In time the environmental conditions could damage textiles (materials/ artifacts) causing the need to develop better non-destructive or at least micro-destructive analysis techniques of the samples. There are ethnographic textile artifacts that were treated in the past with various pesticides, that have not been mentioned in any document. These are often re-treated with chemicals by museum staff as a method of preventing pest infestation. Due to the progressive use of many pesticides, this paper was focused on the detection and quantification of three pesticides: malathion, methoxychlor, and permethrin (cis- and trans- isomers). Gas chromatography is one of the most widely used analytical techniques for characterizing volatile organic compounds and therefore was the analytical method of choice for the present study. Because these analytes are found at trace levels, the detection and quantification limits of analytes are very small and it is necessary to optimize and validate a SIM method - that allows the mass spectrometer to detect specific compounds with high sensitivity. In SIM mode, the instrument is set to collect data at selected masses of interest, thus increasing the accuracy and precision of the quantitative results. The present paper is aimed to develop this type of method with specificity and selectivity, high precision (expressed in terms of repeatability and intermediate accuracy), accuracy, suitable working range and linearity, and high degree of series’ homogenity.

Keywords:
SIM method; gas-chromatography; pesticide; textile

Issue: 2021 Volume 58, Issue 3

Pages: 1-10

Publication date: 2021/10/5

https://doi.org/10.37358/MP.21.3.5498

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This article is published under the Creative Commons Attribution 4.0 International License

Citation Styles

Cite this article as:
MITRAN, E., SANDULACHE, I., LITE, C., RADU, L.G., Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides, Mater. Plast., 58(3), 2021, 1-10. https://doi.org/10.37358/MP.21.3.5498

Vancouver
Mitran E, Sandulache I, Lite C, Radu LG. Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides. Mater. Plast.[internet]. 2021 Jul;58(3):1-10. Available from: https://doi.org/10.37358/MP.21.3.5498

APA 6th edition
Mitran, E., Sandulache, I., Lite, C. & Radu, L.G. (2021). Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides. Materiale Plastice, 58(3), 1-10. https://doi.org/10.37358/MP.21.3.5498

Harvard
Mitran, E., Sandulache, I., Lite, C., Radu, L.G. (2021). 'Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides', Materiale Plastice, 58(3), pp. 1-10. https://doi.org/10.37358/MP.21.3.5498

IEEE
E. Mitran, I. Sandulache, C. Lite, L.G. Radu, "Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides". Materiale Plastice, vol. 58, no. 3, pp. 1-10, 2021. [online]. https://doi.org/10.37358/MP.21.3.5498

Text
Elena-Cornelia Mitran, Irina-Mariana Sandulache, Cristina-Mihaela Lite, Lucian Gabriel Radu,
Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides,
Materiale Plastice,
Volume 58, Issue 3,
2021,
Pages 1-10,
ISSN 2668-8220,
https://doi.org/10.37358/MP.21.3.5498.
(https://revmaterialeplastice.ro/Articles.asp?ID=5498)
Keywords: SIM method; gas-chromatography; pesticide; textile

RIS
TY - JOUR
T1 - Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides
A1 - Mitran, Elena-Cornelia
A2 - Sandulache, Irina-Mariana
A3 - Lite, Cristina-Mihaela
A4 - Radu, Lucian Gabriel
JF - Materiale Plastice
JO - Mater. Plast.
PB - Materiale Plastice SRL
SN - 2668-8220
Y1 - 2021
VL - 58
IS - 3
SP - 1
EP - 10
UR - https://doi.org/10.37358/MP.21.3.5498
KW - SIM method
KW - gas-chromatography
KW - pesticide
KW - textile
ER -

BibTex
@article{MatPlast2021P1,
author = {Mitran Elena-Cornelia and Sandulache Irina-Mariana and Lite Cristina-Mihaela and Radu Lucian Gabriel},
title = {Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides},
journal = {Materiale Plastice},
volume = {58},
number = {3},
pages = {1-10},
year = {2021},
issn = {2668-8220},
doi = {https://doi.org/10.37358/MP.21.3.5498},
url = {https://revmaterialeplastice.ro/Articles.asp?ID=5498}
}

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